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Introduction to Basic Laboratory Equipment

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Chemistry Experiment- Introduction to Basic Laboratory Equipment

The science laboratory is an environment where basic experimental skills are taught through the systematic performance of a set of prescribed and properly designed experiments. Students must follow the rules and regulations in the laboratory and be familiar with the general facilities and equipment. The typical science laboratory consists of a working table, some items of common utility, and a storage space for equipment, chemicals, and glassware. Here students learn about preparing, identifying, and estimating chemical substances. The student must know where to get the necessary apparatus and where to place the chemicals before starting an experiment.


Table of Content

  1. Aim 

  2. Theory 

  3. Apparatus required

  4. Procedure 

  5. Observation 

  6. Result 

  7. Precautions


Aim

To give an introduction to the basic laboratory equipment.


Theory

All the chemistry lab equipment serves different purposes. For example, test tubes can be used to store and mix reagents during chemical reactions, beakers can be used for storing, heating, or mixing substances. Measuring cylinders are narrow cylindrical-shaped instruments used for measuring liquid volumes, and wire gauzes are used to hold flasks or beakers while heating.


Apparatus Required

  • Working table

  • Fume cupboard

  • Side Shelves

  • Exhaust Fans

  • Balance Room

  • Test tubes

  • Beakers

  • Funnel

  • Conical flask

  • Measuring cylinder

  • China dish

  • Glass rod

  • Tripod Stand

  • Wire gauze

  • Bunsen burner

  • Wash bottles


Procedure

Students must familiarise themselves with the following fittings in chemistry laboratories.


  • Students working table: Concrete or wooden tables are given for work. Each seat contains: 

    • Sinks and Water Taps: Every two reagent shelves have a sink and a water faucet. Two taps on either side of the sink usually supply water.

    • Reagent Shelves: Reagents used in the laboratory are placed on the reagent shelf. For example, acids such as HCl, H2S04, HN03, etc., and bases like NH4OH, NaOH, etc. 

    • Gas Taps: These are fitted on the seats for gas supply to the burners.


  • Fume Cupboard: The laboratory includes at least one fume cupboard where experiments release harmful gases or vapours.

  • Side Shelves: Two large shelves are provided on the laboratory's walls. Chemicals and reagents are not frequently used and are put on these shelves. Sometimes, solid chemicals may be placed on a different shelf.

  • Exhaust Fans: Two exhaust fans are provided at the laboratory's two comers to remove poisonous gases and vapours from the laboratory.

  • Balance Room: In this room, a collection of balances is used for weighing the substances in each laboratory.


Common Lab Instruments Name List:

  • Test tubes are usually cylindrical glass pipes with circular openings on one side and rounded bottoms on the other. They are available in different sizes, but the most common is 18x150 mm. A test tube is one of the most important apparatuses since it can store and mix reagents during chemical reactions.

  • Beakers: Glass beakers have a flat bottom, an upper opening, and a spout or no spout, and they come in various sizes. The beakers can be of different sizes and are used for storing, heating, or mixing substances.

  • Funnel: The funnel is necessary for pouring substances and solutions into conical flasks and narrow-mouthed test tubes. Filters, thistles, and dropping funnels are the most common types.

  • Conical flask: The conical flask is cylindrical with a flat circular bottom.  Since it is mostly used in titrations, it is also called a titration flask.

  • Measuring cylinder: Measuring cylinders are narrow cylindrical-shaped instruments for measuring liquid volumes. Each marked line on the graduated cylinder symbolises the measured volume of liquid.

  • China dish: A china dish, also known as the evaporating dish, is made of porcelain. China dishes are thick and come in different sizes. Since they are insulators and can resist higher temperatures, they are used for crystallisation, evaporation, and boiling.


Laboratory apparatus

Laboratory apparatus


Laboratory apparatus (Test tubes, beaker, funnel, conical flask, measuring cylinder, China dish)

Laboratory apparatus (Test tubes, beaker, funnel, conical flask, measuring cylinder, China dish)


  • Glass rod: A glass rod is an object used for mixing. When decanting supernatants, stir rods are used because they form a contact between the supernatants' surface and the side of the glassware, preventing the liquid from running down the side.

  • Tripod stand: A tripod stand consists of three legs and helps to place beakers, flasks, or china dishes.

  • Wire gauze: Wire gauze is a net-like, thin metal sheet placed on the tripod stand to hold flasks or beakers while heating.

  • Bunsen burner: Bunsen burners create a single flame for sterilisation, combustion, and heating.

  • Wash Bottle: A squeezing bottle with a nozzle for rinsing lab apparatus such as flasks and test tubes. The liquid inside the bottle becomes pressurised and is forced through the nozzle when pressure is applied.

  • Practical Notebook: Every experiment should be noted down in a practical notebook. Students must maintain regularity in the practical notebook, which should always have

    • The experiment name and the particular date. 

    • Apparatus required and the principle of the experiment. 

    • The procedure of the experiment, along with observations and results.


Some other apparatuses are required in a chemistry laboratory, such as test tube brushes, test tube holders, spatulas, crucible tongs, clamp stands, watch glasses, pipettes, burettes, water baths, a centrifuge, and a sand bath.


Instructions to Work in Laboratory

  • Ensure that all the chemistry lab apparatus is thoroughly cleaned before use. 

  • Be careful handling the glass apparatus, and immediately inform your teacher if any part breaks. 

  • Allow water to run for a while by opening the water tap after disposing of all waste liquids in the sink. 

  • Make sure your seat is clean, and if corrosive chemicals are spilled, wash them off with water.

  • As soon as you have completed your laboratory work, wash your hands with soap.


Observation

Different chemistry laboratory apparatus and their uses with pictures are observed.


Result

With the help of the following experiment, students can easily recognize different laboratory equipment and understand the instructions to be followed before experimenting.


Precautions

  • In the chemistry laboratory, you should always wear an apron, an eye protector, and a pair of gloves. 

  • As some chemicals are corrosive, do not touch them with your hands.

  • You should always read the label on any reagent or chemical before using it and never use an unlabeled one. 

  • The flame should not be exposed to inflammable liquids like alcohol or ether. 

  • It is always advisable to add acid to the water and not water to acids. 

  • Heating or adding reagents should never be done with the test tube pointed toward yourself or your neighbours. 

  • Always fan chemicals or vapours gently towards your nose when you smell them.


Lab Manual Questions

1. What is the use of wire gauze in a laboratory?

Ans: Wire gauze is a net-like, thin metal sheet placed on the tripod stand to hold flasks or beakers while heating. Since we cannot heat glass apparatus directly in the flame, we use wire gauze to hold them.


2. What is the first aid treatment if you get acid in the eyes?

Ans: If we get acid in the eyes, we should wash the eyes with clean water and then with sodium bicarbonate (1%) solution and again wash with clean water.


3. Why do we need a fume cupboard in a laboratory?

Ans: A fume cupboard is required in a laboratory to conduct experiments releasing harmful gases or vapours.


4. We should not smell chemicals directly. Why?

Ans: Some chemicals may have hazardous effects on our health. Some reagents may irritate the nose, eyes, lungs, and throat. So we should not smell them directly.


Viva Questions

1. Why do we need a wash bottle in a laboratory?

Ans: Wash bottle is required to produce a thin water stream to wash and transfer a precipitate.


2. Which chemical do you apply if you get a minor cut on your hand?

Ans: Methylated spirit is used for the minor cut on the hand.


3. Which equipment is used during filtration?

Ans: A funnel is used during filtration.


4. What is the use of a tripod stand?

Ans: Tripod stand can be used to support a beaker or a china dish while heating on a flame.


5. Which flame is used for the charcoal cavity test?

Ans: Luminous flame is used for the charcoal cavity test.


6. What are the metals used to make wire gauze?

Ans: Iron, copper, nichrome, or steel can be used to make wire gauze.


7. Why do you wear an apron in a chemistry laboratory?

Ans: Aprons protect our clothes from stains or spills. Aprons keep us protected against acids and corrosive chemicals.


8. What do you apply to your skin if you get a burn wound?

Ans: Burnol or mustard oil can be applied on a burn.


9. Which apparatus is used in volumetric analysis to carry out titration

Ans: Conical flask is used in volumetric analysis to carry out the titration.


10. What is the application of a crucible tong?

Ans: A crucible tong is used to hold crucibles, flasks, small beakers, or China dishes that are hot.


Practical-Based Questions

  1. Which apparatus is used for measuring liquid volumes?

A) Conical flask

B) Measuring cylinder

C) Burette

D) Centrifuge

Ans: B) Measuring cylinder


  1. Which of the following chemical is used to wash the eyes if you get alkali in the eyes?

A) Boric acid

B) Nitric acid

C) Sodium hydroxide

D) Hydrochloric acid

Ans: A) Boric acid


  1. Which of the following apparatus is used to stir a liquid mixture?

A) Spatula

B) Glass rod

C) Test tube

D) Pipette

Ans: B) Glass rod


  1. China dish is made of ____.

A) Glass

B) Silver

C) Aluminum

D) Porcelain

Ans: D) Porcelain


  1. Which part of a burner is used to regulate the air supply?

A) Glass inlet tube

B) Burner tube

C) Air regulator

D) Base

Ans: C) Air regulator


  1. Which first aid treatment should be given if someone swallows caustic alkali??

A) Drink a lot of water

B) Drink lemon juice

C) Drink orange juice

D) All the above

Ans: D) All the above


  1. Which instrument is used to separate different fluids based on their densities?

A) Colorimeter

B) Centrifuge

C) Spectrometer

D) None of the following

Ans: B) Centrifuge


  1. Which apparatus is used to remove the poisonous gases from the laboratory?

A) Exhaust fans

B) Fume cupboard

C) Side Shelves

D) Table fans

Ans: A) Exhaust fans


  1. Bunsen burners create a single flame that is used for 

A) Sterilization

B) Combustion

C) Heating

D) All the above

Ans: D) All the above


  1.  Generally, a spatula is made up of which material?

A) Plastic

B) Copper

C) Stainless steel

D) Aluminum

Ans: C) Stainless steel


Conclusion

The student must know where to get the necessary apparatus and where to place the chemicals before starting an experiment. All the chemistry lab equipment serves different purposes. The conical flask is a cylindrical flask with a flat circular bottom.  Since it is mostly used in titrations, it is also called a titration flask. Wire gauze is a net-like, thin metal sheet placed on the tripod stand to hold flasks or beakers while heating. In the chemistry laboratory, you should always wear an apron, an eye protector, and a pair of gloves.

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FAQs on Introduction to Basic Laboratory Equipment

1. What are the safety apparatuses required in a chemistry laboratory?

Disposable gloves, safety goggles to protect the eyes, aprons, fire extinguishers, first aid kits, chemical spill kits, eye wash stations, emergency showers, chemical fume hoods, and safety storage cabinets are some of the important safety apparatus required in a chemistry laboratory.

2. What are the common laboratory safety measures?

It is not advisable to touch the chemicals, even though they are not corrosive, because some chemicals may cause skin allergies or other problems. Since many of the solvents are toxic and can cause nose, eyes, and throat irritation, it is better not to inhale them. Since some chemicals may be flammable, one should be aware of them.

3. What is the use of goggles in a chemistry laboratory?

Laboratory space is common for eye injuries, which can be very serious. Wearing goggles can help prevent eye injuries. Chemists use goggles routinely to protect against chemical splashes, concentrated corrosive materials, and bulk chemical transfers. Some goggles may suit the lenses as well.